@nanographs@chaos.social
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nanographs

@nanographs@chaos.social

Electron microscopes ❤️ open hardware

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nanographs, to random
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I think it’s possible I’m the first person to be doing dual beam alignments via an iPad (Sidecar).

Unexpected benefits of the Open Beam Interface for the win! The main monitor is facing away from the microscope, but I can just walk around with my iPad to wherever I need to be.

nanographs, to random
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Doorstops in Sánchez lab be like

nanographs, to random
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We have completed our first Open Beam Interface installation!

Dr. Adam Summers lab at the University of Washington Friday Harbor Marine Biology Labs is now capturing 16x larger scans than was possible before.

Big milestone for us, first time delivering our open source hardware to a customer.

Get in touch if you too want us to upgrade your SEM.

Picture of the front of the SEM with the open beam interface software running on an iMac
Picture of the open beam interface circuit board on the back of a SEM, many orange labels on all of the cables.

nanographs,
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We also significantly improved the microscope control computer situation.

It started out as an un-networkable XP then 7 box.

We got the JEOL SEM software running on windows 10 through some driver configuration, then setup Remote Desktop from the iMac into the windows 10 box.

nanographs,
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We published some notes on how we installed it on the NEOScope. It was a bit cramped in there so took some fancy soldering. We could (if we got the crimp tooling) make cables and PCBs that would enable this to be done with no soldering required.

https://datacore.nanographs.io/000+Publish/Neoscope+OBI+Installation

nanographs,
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@penguin42 yeah exactly, now that we have the pinouts and information on the connectors.

nanographs, to random
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Talking to some other microscope engineers about the cables we are making and how much machined (as opposed to stamped) contacts for small gauge wires cost:
"What are the contacts made out solid gold?"
"No they are only coated in 30µm"

nanographs, to random
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This is a relay diagram.

They take us for fools.

nanographs, to random
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Used a sphere of plastic and the Open Beam Interface to capture Electron Microscope selfies on our JEOL JSM 6400 SEM from the 80s.

I charged the sphere with a 20kV beam, then dropped the beam energy to 3kV to bounce the beam off the sphere and image the inside of the SEM.

The hole in the center of the frame is the bottom of the column and where the beam came from. The springs and linkages around the edge of the frame is the SEMs stage.

nanographs, to random
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Spinning a Glasgow to M8 breakout for us to connect microscope blanking and scan selectors to.

nanographs, to random
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Hey anyone here decent with magnets field simulations in COMSOL? Helping a friend find someone for a paid consulting gig.

nanographs, to random
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Stood up our new Open Beam Interface gateware with
@whitequark and @isabel tonight. These are most of the images it took to debug the new gateware.

nanographs,
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@mcc @whitequark @isabel Haha yeah it’s the holy cross of thermal isolation. This thermal cameras happened to be the last sample in the SEM when we stared testing the gateware: https://chaos.social/@nanographs/112017449965727177

nanographs, to random
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Introducing the first open source SEM digital image capture solution, the Open Beam Interface!

GitHub: https://github.com/nanographs/Open-Beam-Interface

Bring your analog SEM into the digital world, all over one USB type-C connection.

Taking orders now for our first batch of 6 boards, DM for details.

FIB image of a diatom with a chunk cut away
FIB image if a MEMS microphone
FIB image of an ICE40 with a large trench cut in it

nanographs, to random
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Captured some scans under the SEM and FIB of the AMG8833 Grideye 8x8 thermal camera using our Open Beam Interface.

The FIB milled out the rectangle, revealing in cross section wires looping around forming a thermistor. Under each pixel is a KOH etched void for thermal isolation.

Medium mag SEM image showing the corner of one of the pixels, and a rectangular cross section of a trench.
High mag FIB image of the cross section showing the wires buried under a layer of silicon, and a void behind the pixel.

nanographs, to random
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TFW you work on electron microscope controls with @whitequark and she immediately turns it all into a compiler problem. Watching her write Amaranth is something else, @isabel and I learned a ton!

https://mastodon.social/@whitequark/111987067448322106

nanographs, to random
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Realized that we haven't yet come across an old SEM that we didn't get into a good shape in about 2 weeks (except the one I got in high school), looking at offering this as a service.

Also, we have folks trying to re-home some JEOL 840s right now, so here's what we're thinking:

Picture of a JEOL 840 with a Diatom on screen
Picture of water cooled electronics bay with many colored wires
Picture of stage, poll piece, and back scatter detector inserted

nanographs,
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Buy an JEOL 840, have us move it/tune it up for you:

  • 840: 4-10k
  • Packing: 2-5k
    Shipping: 2-5k
    2 week of me and @beamshift
    at your site for tune up: 10-14k
    Open Beam Interface image capture hardware: ~2k
    Total: 20k - 38k

We do the work with you, teaching you about the scope.

Picture of the electron source and anode
Picture of the electron source open
Picture of the sample load lock in opperation

nanographs, to random
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nanographs, to random
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Used an ICE40 to FIB mill a big hole (the size of a small hole) in an ICE40.

nanographs, to random
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Came in and started up on of our SEMs and had a classic "whats that burning smell investigation...

Pretty sure its "normal" but wrote a post about it. Long story short there is a resistor heating up to (gasp) 650°F!

https://datacore.nanographs.io/000+Publish/6400+CRT+1+Balast+Resistor+Heating

nanographs, to random
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Open hardware, coming soon to a (electron or other) microscope near you.

North, to random
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So... it took until I received my $80 chunk of stainless steel from Duniway to realize that my deep discount ion gauge is actually not 0.75" tubulated. Despite there being no part# that I can find for a 0.5" tubulated gauge, that's what this appears to be.

The good news is, that makes it compatible with the MUCH cheaper and more common 15.5mm ion gauge adapters. Besides, I'll get some use out of this 0.75" adapter down the road.

Everyone join me in admiring the expensive nugget.

nanographs,
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@North only 80$ for anything from duniway is impressive

azonenberg, to random
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The now-very-crowded optics bench. I definitely need to spend some time over Christmas vacation tidying up the lab.

nanographs,
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@azonenberg do you use the throttle for focus

breakingtaps, to random

Lithography is hard, but litho over a centimeter is really hard! 😅

Test photomask for 10:1 reduction. Stitching, normalizing exposures, development, etching. Was a battle to get it all working but starting to get there.

Can see the stitch misalignment every 400µm. Errors are ~3µm, so 300nm at final resolution. Min feature is 2µm, so in theory it should be ok 🫣

image/jpeg
image/jpeg
image/jpeg

nanographs,
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@breakingtaps @azonenberg @gom

What resolution can the bmp for EBL be?

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